The corresnonding imines were obtained by working-up aldimmonium salts with triethylamine. The 2-O,O-dialkyldithiophosphatopropanals were synthesized by hydrolysis of imines and their salts. The aldehydes were transformed into acetals, 2,4-dinitrophenylhydrazone and hydrazone of diphenylphosphinylacetic acid hydrazide.
соли 2-О,О-диалкилдитиофосфатоальдиммония, 2-О,О-диалкилдитиофосфатопропанали, триалкилортоформиаты, ацетали, гидразин, гидразид, гидразоны, спектры ЯМР 1H и 31Р, 2-О,O-dialkyldithiophosphatoaldimmonium salts, 2-O,O-dialkyldithiophosphatopropanals, trialkylorthoformates, acetals, hydrazine, hydrazide, hydrazones, 1H, 31Р NMR spectra
1. Gazizov M.B. Reakcii O-metildietiltiofosfinata s arilidenhloridami / M.B. Gazizov, G.D. Valieva, L.R. Bagauva, O.D. Hayrullina, R.F. Karimova // Vestnik Kazan. tehnol. un-ta.-2012.-T. 15.- №4.- S.10-12
2. Gazizov M.B. Reakcii S-metildietiltiofosfinata s ariliden hloridami / M.B. Gazizov, G.D. Valieva, L.R. Bagauva, R.K. Ismagilov, G.F. Karimova, S.Yu. Ivanova // Vestnik Kazan. tehnol. un-ta. - 2012.-T.15, №6.-S.7-9
3. Gazizov Mukattis B. New products of the reaction of aldimines with dialkylphosphites / Mukattis B. Gazizov, Rafail A. Khairullin, Anastasya I. Alehina, Igor A. Litvinov, Dmitrii B. Krivolapov, Shamil K. Latipov, Alsu A. Balandina, Rashid Z. Musin, Oleg G. Sinyashin // Mendeleev Commun. 2008.-V18.- P. 262-264
4. Gazizov M.B. Vzaimodeystvie dialkilfosforistyh kislot s N-alkil- 2-hloral'degidiminami / M.B. Gazizov, R.A. Hayrullin, A.A. Minnihanova, A.I. Alehina, A.A. Bashkircev, O.G. Sinyashin //Doklady RAN.-2012.-T.433, №3.-S.1-5
5. Gazizov Mukattis B. Phosphorylated aziridium salts: synthesis and ring opening with nucleophiles / Mukattis B. Gazizov, Pafail A. Khairullin, Alina A. Minnikhanova, Anastasya I. Alekhina, Rashid Z. Musin, Oleg G. Sinyashin // Mendeleev Commun. 2011.-V21.-P. 1-3
6. Gazizov M.B. Reakcii dialkilfosforistyh kislot s N-alkil-2-hloral'diminami / M.B. Gazizov, R.A. Hayrullin, A.A. Minnihanova, A.I. Alehina, A.A. Bashkircev // Vestnik Kazan. tehnol. un-ta.-2010, №5. S.55-59
7. Gazizov Mukattis B. Reaction of Dialkylphosphites with N-alkyl-2-chloroaldimines / M.B. Gazizov, R.A. Khairullin, A. A. Minnikhanova, A.I. Alehina, A.A. Bashkirtsev, O.G. Sinyashin // Russian Journal of General Chemistry. - 2012.-V. 80, №12.-R. 2425-2429
8. Zimin M.G. O vzaimodeystvii ditiokislot fosfora s benzal'anilinom i benzal'metilaminom / M.G. Zimin, N.G. Zabirov, R.A. Cherkasov, A.N. Pudovik // ZhOH. -1978.- T.48, №5.-S. 1020-1025.
9. Zimin M.G. Reakcii ditiokislot fosfora s soedineniyami, soderzhaschimi kratnye svyazi uglerod-azot / M.G. Zimin, N.G. Zabirov, R.A. Cherkasov, A.N. Pudovik // ZhOH.-1980.-T.50, №7.-S.1458-1463
10. Hayrullin R.A. Reakcii N-tret-butil-2-hloral'dimina s O,O-dialkilditiofosfornymi kislotami / R.A. Hayrullin, M.B. Gazizov, N.G. Aksenov, O.I. Gnezdilov // Vestnik Kazan. tehnol. un-ta.-2013.- T.16, № - S.
11. De Kimpe N. The Synthesis of α- halogenated imino Compounds / N. De Kimpe, N. Schamp // Organic Preparation and Procedures Int.-1979.-V. 11, Issues 3-4.-P.115-199
12. De Kimpe N. Reactivity of α-halogenated imino Compounds N. De Kimpe, D.B. Laurent, N.Schamp // Organic Preparation and Procedures Int.-1980. V.12, Issues 1-2.-P. 49-180
13. Iorga B. Phosphorylated Aldehydes: Preparation and Synthetic Uses / Iorga, F. Eymery, V. Mouries, Ph. Savignac // Tetrahedron: Pergamon.-1954.-V.54.- P. 14637-14677
14. Razumov A.I. Fosforilirovannye al'degidy / A.I. Razumov, G.G. Lior'er, V.V. Moskva, M.P. Sokolov // Uspehi himii.-1973.-T.42, Vyp.7. -S. 1199-1224
15. Michalski J. Reaction of dialkoxyoxophosphorane-sulphenyl chlorides with enol esters and esters / J. Michalski, S. Musierowicz // Chem. and Ind.-1959.- P.565