This article describes the synthesis of various urea derivatives containing 4,4-diethoxybutan-1-amine moiety. Structures of products were confirmed by NMR 1H, 31P, IR-spectroscopy and elemental analysis.
аминоацеталь, мочевина, цианат натрия, фенилизотиоцианат, aminoacetal, urea, sodium cyanate, phenyl isothiocyanate
1. Vagapova L.I., Gazizov A.S., Burilov A.R., Harlampidi H.E., Pudovik M.A. Sintez novyh tiofosforilirovannyh tiomochevin, soderzhaschih v soctave acetal'nuyu gruppu. Vestnik KGTU. 2012, T.17, S.26-29.
2. Vagapova L.I., Pavlova E.Yu., Burilov A.R. Issledovanie vzaimodeystviya fosforilirovannogo aminoacetalya s 2-metilrezorcinom. Vestnik KGTU. 2013, T.17, №4, S.56-57.
3. Burilov, A. R.; Khakimov, M. S.; Gazizov, A. S.; Pudovik, M. A.; Syakaev, V. V; Krivolapov, D. B.; Konovalov, A. I. Mendeleev Commun. 2008, 18, 54-55.
4. Smolobochkin A. V., Gazizov A. S., Vagapova L. I., Burilov A. R., Pudovik M. A. Vzaimodeystvie 1-(4,4-dietoksibutil)mocheviny s rezorcinami. Sintez novyh 2-arilpirrolidinov. Izv. AN. Ser. him. - 2014, -№1, - S. 284-285.
5. Vishnyakova T. P. Zameschennye mocheviny, metody sinteza i oblasti primeneniya / Vishnyakova T. P., Golubeva I. Α., Glebova E. V. // Uspehi himii. - 1985. - T. LIV. - Vyp. 3. - S. 629-449.
6. Peng L., Zhiming W., and Xianming H. Highly Efficient Synthesis of Ureas and Carbamates from Amides by Iodosylbenzene-Induced Hofmann Rearrangement. Eur. J. Org. Chem. 2012, 1994-2000.
7. Khakimov M.S. Reaction of Resorcinol and Its Derivatives with Urea Acetals / M. S. Khakimov, A. S. Gazizov, A. R. Burilov, M. A. Pudovik, and A. I. Konovalov // Russian Journal of General Chemistry. - 2009. - Vol. 79, No. 6, pp. 1163-1166.
