This article provides an overview of the existing methods for determining accredited heavy metals in the air with the use of instrumental methods of analytical chemistry, including physical and physico-chemical methods for determining that allow for both qualitative and quantitative determination . This process is time consuming as it requires a lot of time for testing , skilled staff , and the cost of such analysis is quite high . Therefore, the authors propose to use a combination of computational and experimental control methods with preliminary identification of metal markers that will create a model of pollution , followed by analysis in accredited laboratories , if necessary , to reduce the time and cost.
тяжелые металлы, контроль атмосферного воздуха, методическое обеспечение, heavy metals, control of air, methodological support
1. O.S. Egorova, E.V. Gogol', R.R. Shipilova, Yu.A. Tunakova, Vestnik KTU, 16, 19, 71 - 75 (2013).
2. O.M. Cherp, V.N. Vinichenko, Problema tverdyh bytovyh othodov: kompleksnyy podhod. Ekolayn, Moskva, 1996.
3. I.Novikova, Tualety, komposty, utilizaciya othodov. Veche, Moskva, 2005. 192 s.
4. Vtorichnaya pererabotka polimerov i plastmass [Elektronnyy resurs]. (http://www.polimech.com/home/artcles/vybor.html).
5. A.M. Prohorov, Bol'shaya Sovetskaya Enciklopediya. (V 30 tomah). T. 19. Sovetskaya Enciklopediya, Moskva, 1975. 648 s. s ill.
6. Mirovoy rynok krasiteley dlya polimerov [Elektronnyy resurs]. (http://www.newchemistry.ru).
7. V.V. Kurilenko, I.I. Podlipskiy, Sistema upravleniya bytovymi othodami v Rossii: ekologicheskie problemy i metody utilizacii [Elektronnyy resurs]. (http://www.burim24.ru/stat'i/sistema-upravleniya-bytovymi-othodami)
8. Yu.S. Drugov, A.B. Belikov, G.A. D'yakova, V.M. Tul'chinskiy, Metody analiza zagryazneniy vozduha. Himiya, Moskva, 1984. 384 s., il.
9. A.P. Kreshkov, Osnovy analiticheskoy himii. Fizicheskie i fiziko-himicheskie (instrumental'nye) metody analiza. Himiya, Moskva, 1977. 486 s.
10. V.P. Vasil'ev, Analiticheskaya himiya. Fiziko-himicheskie metody analiza. Vysshaya shkola, Moskva, 1989. 384 s.
11. Yu.A. Zolotov, E.N. Dorohova, V.I. Fadeeva i dr., Osnovy analiticheskoy himii. Vysshaya shkola, Moskva, 2004. 361 s.
12. T.N. Shehovcova, S.V. Muginova, I.A. Veselova, Zhur. Ros. him. ob-va im D.I. Mendeleeva, XLVIII, 4, 73 - 82 (2004).
13. Kineticheskie i fermentativnye metody [Elektronnyy resurs]. (http://khimie.ru/analiticheskaya-himiya/kineticheskie-i-fermentativnyie-metodyi)
14. B. Krajewska, A. Leszko, W.J. Zaborska, Chem. Technol. Biotechnol., 48, 337-350 (1990)
15. H. Weisz, K. Rothmaier, Anal. Chim. Acta, 80, 2, 357-359 (1975)
16. E.C. Toren, F.J. Burger, Mikrochim. Acta, 5, 1949 (1968)
17. D. Mealor, A. Townshend, Ibid., 15, 12, 1371 (1968)
18. J. Maslovskaya, T. Leszczynnskay, Talanta, 32, 9, 883-886 (1985)
19. E.C. Toren, F.J. Burger, Mikrochim. Acta, 3, 538 (1968)
20. G.G. Guilbault, D.N. Kramer, P.L Carron, Anal. Chem., 36, 3, 606-610 (1964)
21. A. Townshend, A. Vaughan, Talanta, 17, 4, 299 (1970)
22. A. Townshend, A. Vaughan, Talanta, 16, 7, 929 (1969)
23. G.B. Slepchenko, N.P. Pikula, N.M. Dubova, T.I. Schukina, O.S. Zharkova, Izvestiya Tomskogo politeh. un-ta, 314, 3, 59 - 70 (2009)
24. F. Vydra, K. Shtulik, E. Yulakova, Inversionnaya vol'tamperometriya. Mir, Moskva, 1980, S. 257 - 265
25. P. R. Harrison, J. W. Winchester, Atmospheric Environment, 5, 863 (1971)
26. E.O. Averyaskina, S.S. Ermakov, L.N. Moskvin, VII konferenciya "Analitika Sibiri i Dal'nego Vostoka - 2004" (Novosibirsk, Rossiya, 11-16 oktyabrya, 2004). Novosibirsk, 2004.
27. Oficial'nyy sayt nauchno-proizvodstvennoy kompanii «Akvilon» [Elektronnyy resurs]. (http://www.akvilon.su)
28. H.Z. Braynina, E.Ya. Neyman, V.V. Slepushkin, Inversionnye elektroanaliticheskie metody. Himiya, Moskva, 1988. 239 s.
29. V.N. Maystrenko, Ekologo-analiticheskiy monitoring supertoksikantov. Himiya, Moskva, 1996. 319 s.
30. RD 52.04.186-89. Rukovodstvo po kontrolyu zagryazneniya atmosfery. Goskomgidromet SSSR, Moskva, 1991. 693 s.
31. Sbornik metodik po opredeleniyu koncentraciy zagryaznyayuschih veschestv v promyshlennyh vybrosah. Gidrometeoizdat, Leningrad, 1987.270 s.
32. O.V. Kuznecova, E.N. Korzhova, A.N. Smagunova i dr., Zhurn. analit. himii, 59, 1, 46 - 51 (2004)
33. V.K. Karandashev, A.N. Turanov, T.A. Orlova i dr., Zavodskaya laboratoriya, 73, 1, 12 - 22 (2007)
34. J. Tolgyessy, L. Olah, E.H. Klehr, J. Radioanal. and Nucl. Chem., 114, 1, 101 - 104 (1987)
35. M. Matherny, H. Niekel, Euroanalysis 5: 5th Eur. Conf. Anal. Chem. (Krakow, Polska, 1987). Book Abstacts. Krakow, 1984. R. 313
36. V.A. Mihaylov, S.G. Pushkin, A.A. Nazarov i dr., V sb. tr. Zap. - Sib. Regional'nogo nauchno-issledovatel'skogo gidrometeorologicheskogo instituta. 1979. S. 40
37. T.V. Latypova, E.V. Petrova i dr., Vestnik TGASU, S. 138 - 147 (2008)
38. Gidrometeorologiya. Ser. «Kontrol' za zagryazneniyami prirodnoy sredy». Obzornaya informaciya. Goskomgidromet SSSR, Obninsk, vyp. 4, 1982. 35 s.
39. R.D. Ediger, D.W. Hoult, Atom. Spectrosc., 1, 2, R. 41 (1980)
40. J. Cormic & e.a., Abstr. Pap. presented Pittsburgh Conf. and Expo. Anal. Chem. and Appl. Spectrosc. (New York, Atlantic City, 1982). New York, 1982. R. 653
41. A. Sugimae, T. Mizoguchi, Anal. chim. acta, 144, 2, R. 205 (1982)
42. C. Gangadhar, Chemical Hazarda in the Workplace. Measurement and Control. Ass Symp. Ser. 149, Washington, 1981.
43. A.S. Alemasova, A.N. Rokun, I.A. Shevchuk, Analiticheskaya atomno-absorbcionnaya spektroskopiya. Doneck, 2003. 327 s.
44. D.L. Fox, H.E. Jeffries, Anal. Chem., 53, 5, 1 (1981)
45. M.E. Bricke, Atomno-absorbcionnyy spektrohimicheskiy analiz. Himiya, Moskva, 1982
46. D.L. Fox, H.E. Jeffries, Anal. Chem., 55, 5, 233 (1983)
47. J.E. Hwang, Anal. Chem., 44, 14, 2140 (1972)
48. W. Jonghe, F. Adam, Anal. Shim. acta, 108, 1, 21 (1979)
49. F. Slemr & e.a., Anal. Shim. acta, 110, 1, 35 (1979)
50. G. Holzer & e.a., J. Chromatogr., 142, 2, 755 (1977)
51. W. Averill, J.E. Purcell, 29th Pittsburh Conf. Anal. Chem. and Appl. Spectrosc. (Cleveland, Ohio, 1978). Abstacts. Cleveland, 1978. R. 441
52. A.V. Kiselev, Ya.I. Yashin, Gazoadsorbcionnaya i zhidkostnaya hromatografiya. Himiya, Moskva, 1979
53. R.E. Cullen, M.T. Michand, Amer. Ind. Hyg. Assoc. J., 39, 8, 684 (1978)
54. Metodicheskie ukazaniya po opredeleniyu vrednyh veschestv v svarochnom aerozole, Moskva, 1992
55. ISO 9855, 8515
56. L.V. Osipova. Avtoref. diss. kan. teh. nauk, Sankt-Peterburgskiy gos. un-t, Sankt-Peterburg, 2001.
57. S. Kataev. Hromato-mass-spektrometriya [Elektronnyy resurs]. (http://www.chromatec.ru)
58. E. Gard, J.E. Mayer, B.D. Morrical, D.P. Fergenson, K.A. Prather, Anal. Chem., 69, 4083 (1997)
59. C.-J. Chin, C.-F. Wang, S.-L. Jeng, J. Anal. At. Spectrom., 14, 663 (1999)
60. V.K. Karandashev, S.A. Sklovski, D.V. Kaplun, Colloquium Spectroscopicum Internationale XXXI (Ankara, Turkey, September 5 - 10, 1999). Book of Abstracts. Ankara, 1999. P. 112
61. E.N. Korzhova i dr., Zh. analit. himii, 66, 3, 228 - 246 (2011)
62. E.V. Morozkina, Yu.M. Polezhaev, Analitika i kontrol', 3,4 - 10 (1999)
63. MUK 1618-77. Metodicheskie ukazaniya na fotometricheskoe opredelenie medi v vozduhe. Vyp. 1-5. CRIA «Morflot», Moskva, 1981. 47 s.
64. K.S. Ful'mes, A.V. Bulatov, Yu.M. Dedkov, L.N. Moskvin, Zhurn. Analitika i kontrol', 16, 3, 275 - 280 (2012)
65. Abstracts 17-th Intern. Conf. on Flow Injection Analysis Including Related Techniques (Krakow, Polska, 2011). Krakow, 2011. R. 162
66. Oficial'nyy sayt ekologo-analiticheskogo informacionnogo centra «SOYuZ» [Elektronnyy resurs]. (http://www.center-souz.ru)
67. Oficial'nyy sayt NPO «Krismas-Centr» [Elektronnyy resurs]. (http://www.ccentr.msk.ru)
68. Oficial'nyy sayt NPO «Atmosfera» [Elektronnyy resurs]. (http://www.atmosfera-npk.ru).
