SINTEZ 2-(
                  P-(1-ADAMANTIL)METILFENILTIO)-6-METILPIRIMIDIN-4(3N)-ONA

Titova E S; Rahimov A I; Babkin V A; Ignatov A V; Zaikov G E; Stoyanov O V

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SINTEZ 2-( P-(1-ADAMANTIL)METILFENILTIO)-6-METILPIRIMIDIN-4(3N)-ONA

Journal: HERALD OF TECHNOLOGICAL UNIVERSITY Volume 17 № 13 , 2025

Rubrics: STRUKTURA VESCHESTVA I TEORIYA HIMICHESKIH PROCESSOV

UDC 54.06

Titova E S ¹

Rahimov A I ²

Babkin V A ³

Ignatov A V ⁴

Zaikov G E ⁵

Stoyanov O V ⁶

Author and publication information

Authors:

1. Volgogradskiy gosud. tehnich. un-t; department “Organic Chemistry” of Volgograd State Technical University

2. Volgogradskiy gosud. tehnich. un-t; RAEN; Russian Academy of Natural Sciences. Department “Organic Chemistry” of Volgograd State Technical University

3. RAE, Mezhdunarodnaya akademiya «Kontenant», Sebryakovskiy filial Volgogradskogo gosud. un-ta; international academy “Contenant”, Head of Science department of Volgograd State Architecture Building University, Sebryakov’s Branch

4. Sebryakovskiy filial Volgogradskogo gosud. un-ta; Volgograd State Architecture Building University, Sebryakov’s Branch

5. Mezhdunarodnaya akademiya nauk (Myunhen, Germaniya), Institut biohimicheskoy fiziki, RAN, Moskva; international academy of Science (Munich, Germany), Honored scientist of Russian Federation. Institute of Biochemical Physics, Moscow

6. KNITU; KNRTU

Type:

Article

Pages:

from 12 to 13

Status:

Published

Received:

20.04.2023

Accepted:

01.08.2025

Published:

01.08.2025

Subject area:

UDC 54.06

Language:

Russian

Keywords:

2-(п-(1-адамантил)метилфенилтио)-6-метилпиримидин-4(3Н)-он, нуклеофильное замещение, 2-(para-(1-adamantyl)methyphenyllthio)-6-methylpyrimidin-4(3H)-one, nucleophylic substitution

Abstract and keywords

Abstract (English):
2-(para-(1-Adamantyl)methyphenyllthio)-6-methylpyrimidin-4(3H)-onewas synthesized by nucleophylic substitution reaction of bromine in para-(1-adamantyl)benzylbromid by S-anion, generated from 6-methyl-2-thiouracil.

Keywords:
2-(п-(1-адамантил)метилфенилтио)-6-метилпиримидин-4(3Н)-он, нуклеофильное замещение, 2-(para-(1-adamantyl)methyphenyllthio)-6-methylpyrimidin-4(3H)-one, nucleophylic substitution

References

1. S- i O-aniony, generiruemye iz 6-metil-2-tio-, 2-alkil(aralkil)tiouracilov, v sinteze S-monoi S-,O-dialkil-, benzilproizvodnyh. Titova E.S. dissertaciya na soiskanie uchenoy stepeni kandidata himicheskih nauk/Volgograd, 2005.

2. Osobennosti sinteza 2-alkil(arilalkil)tio-6-metilpirimidin-4(3N)-onov i 2-alkil(arilalkil)tio-4-alkil(arilalkil)oksi-6-metilpirimidinov. Rahimov A.I., Titova E.S. ZhOH. 2007. T. 43. № 1. S. 92-98.

3. Generaciya Si O-anionov iz 6-metil-2-tio-, 2-alkil(aralkil)tiouracilov v sinteze S-monoi S-,O-diproizvodnyh. Rahimov A.I., Titova E.S., Fedunov R.G., Babkin V.A., Stoyanov O. V., Zaikov G.E. // Vestnik Kazanskogo tehnologicheskogo universiteta. - 2013. - T. 16, № 5. - C. 23-29.

4. Nukleofil'noe zameschenie v benzil 1-(hlormetil)-3-fenoksibenzilhloridah s uchastiem 4-metil-6-okso-1,6-digidro-2-pirimidintiolat aniona. Rahimov A.I., Popov Yu.V., Titova E.S. Izvestiya volgogradskogo gosudarstvennogo tehnicheskogo universiteta. 2005. № 1. S. 61 - 64.

5. Sintez simmetrichnyh i nesimmetrichnyh S-,O-diproizvodnyh 6-metil-2-tiouracila. Rahimov A.I., Titova E.S. Izvestiya volgogradskogo gosudarstvennogo tehnicheskogo universiteta. 2006. № 1. S. 66 - 72.

6. Osobennosti nukleofil'nogo zamescheniya v alkil- i benzilgalogenidah anionami, generiruemymi iz 4-gidroksi-2-merkapto-6-metilpirimidina. Rahimov A.I., Titova E.S., Fedunov R.G., Babkin V.A. Himiya geterociklicheskih soedineniy. 2008. № 6. S. 874-883.

7. Rakhimov A.I., Titova E.S. 2007. T. 43. S. 96-102.

8. Reakcionnaya sposobnost' Si O-anionov, generiruemyh iz 6-metil-2-tio-, 2-tioalkil(aralkil)uracilov. Rahimov A.I., Titova E.S., Fedunov R.G., Babkin V.A., Belousova V. S., Rusanova S. N., Zaikov G.E. // Vestnik Kazanskogo tehnologicheskogo universiteta. - 2013. - T. 16, № 5. - C. 16-20.

9. Kvantovo-himicheskiy analiz reakcionnoy sposobnosti S- i O-anionov, generiruemyh iz 6-metil-2-tio-, 2-alkil(aralkil)tiouracilov. Rahimov A.I., Titova E.S., Fedunov R.G., Babkin V.A. Izvestiya volgogradskogo gosudarstvennogo tehnicheskogo universiteta. 2008.T. 1. № 5. S. 70 - 75.

10. Kvantovo-himicheskie issledovaniya mehanizma sinteza 2-metil(benzil)tio-4-metil(benzil)oksipirimidina. Babkin V.A., Rahimov A.I., Titova E.S., Fedunov R.G., Reshetnikov R.A., Belousova V. S., Zaikov G.E. Himicheskaya fizika i mezoskopiya. 2007. T. 9. № 3. S. 263-275.

11. Rahimov A.I., Babkin V.A., Titova E.S., Fedunov R.G., Belousova V.S., Zaikov G.E.V sbornike: sbornik statey: k 59-letiyu so dnya rozhdeniya professora V. A. Babkina. M-vo obrazovaniya i nauki Rossiyskoy Federacii, Volgogradskiy gosudarstvennyy arhitekturno-stroitel'nyy universitet, Serebryakovskiy filial, Kafedra matematiki i estestvennonauchnyh disciplin; pod redakciey V. A. Babkina. Volgograd, 2011. S. 41-50.

12. Sposob polucheniya 1,3-di[4-(6-metil-4-pirimidinon-2-tio)metilfenil]adamantana. Rahimov A.I., Titova E.S. patent na izobretenie RUS 231141211.07.2006.

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